Data for yield and characterisation and performance measurements of UTSA-16 magnetic framework composites synthesised in flow
Publication Date
October 2, 2024
Creators
Description
Data collected herein support the following article and supplementary information: Continuous flow synthesis of MOF UTSA-16(Zn), mixed-metal and magnetic composites for CO2 capture – toward scalable manufacture. Data include: yield and temperature for decomposition (TGA), carbon dioxide adsorption and capture-release cycling (TGA), gas sorption isotherms, mineral liberation analysis, vibrating sample magnetometry, induction heating profiles, scanning electron microscopy (SEM) images, and inductively coupled plasma optical emission spectroscopy (ICP-OES), x-ray diffraction and lab book notes.
Parent projects:
Magnetic framework composites for CO2 capture John Luke Woodliffe PhD project
Coverage (Spatial):
UK
Collection dates:
September 2020 - July 2024
Related resources
Subjects
Subjects (JACS)
Subjects (LC)
Divisions
University of Nottingham, UK Campus::Faculty of Engineering::Department of Chemical and Environmental Engineering
Corporate collaborators
Royce Discovery Centre, The University of Sheffield
Department of Chemistry and Materials Innovation Factory, University of Liverpool
University of Nottingham
Data type
scanning electron microscopy images, heating profiles, gas sorption data, lab book notes, thermogravimetric analysis data, vibrating sample magnetometry data, powder x-ray diffraction, yields, mineral liberation analysis images, inductively coupled plasma optical emission spectra (ICP-OES), gravimetric carbon dioxide sorption data.
Funders
Science Foundation Ireland
Grant Number
Royce Discovery Centre, University of Sheffield; EPSRC Grant Number EP/R00661X/1 & EP/P02470X/1
Engineering and Physical Sciences Research Council (EPSRC) and Science Foundation Ireland (SFI) Centre for Doctoral Training in Sustainable Chemistry: Atoms-2-Products an Integrated Approach to Sustainable Chemistry, Grant number: EP/S022236/1
SEM analyses were supported by the EPSRC (EP/L022494/1) and the University of Nottingham
MLA/EDS analyses were supported by the EPSRC (EP/P006701/1), as part of the “EPSRC Future Composites Manufacturing Research Hub”
Data collection method
powder x-ray data: Bruker D8 Advance DaVinci with a Lynxeye 1D detector (Bragg-Brentano geometry), SEM images: Jeol 7000F FEG-SEM (Jeol PC-SEM software), MLA: Backscattered electron (BSE) imaging and chemical analyses using SEM, FEI Quanta600 based mineral liberation analysis (MLA) equipped with energy dispersive X-ray spectroscopy (EDS) for compositional analysis and linked Bruker/JKTech/FEI data acquisition software for automated mineralogy, TGA data: TA instruments TGA550 Discovery, gravimetric CO2 capture release cycles: TA instruments TGA550 Discovery, N2 and CO2 isotherms: Micromeritics ASAP 2020 V4.04, Vibrating-sample magnetometry (VSM): Quantum Design SQUID MPMS3, heating profiles: Cheltenham Induction Heating Ltd induction heater (2 kW, 204 kHz), Inductively coupled plasma optical emission spectroscopy (ICP-OES) Agilent 5110 Vertical Dual View instrument equipped with 240 place SPS-4 autosampler instrument operation and data processing was via the Agilent ‘ICP Expert’ software package.
Legal and ethical issues
Do not process or publish data without consent
Resource languages
English
Publisher
The University of Nottingham
Date Issued
October 2, 2024
Except where otherwise noted, this item's license is described as
File(s)![Thumbnail Image]()
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Name
TGA thermal decomposition.xlsx
Description
TGA data for thermal decomposition of MOFs and magnetic framework composites
Size
387.78 KB
Format
Microsoft Excel XML
Checksum (MD5)
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Name
MOF TGA CO2 cycles - 60C x12.xlsx
Description
data for TGA CO2 gravimetric capture-release cycles for the MOF
Size
6.89 MB
Format
Microsoft Excel XML
Checksum (MD5)
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